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Enantioselective Total Syntheses of (−)-Cochlearol B and (+)-Ganocin A

  • Tomoya Mashiko,
  • Yuta Shingai,
  • Jun Sakai,
  • Shinya Adachi,
  • Akinobu Matsuzawa,
  • Shogo Kamo,
  • Kazuyuki Sugita

摘要

Herein, we describe the first total synthesis of (±)-cochlearol B and the enantioselective total syntheses of (−)-cochlearol and (+)-ganocin A. The key steps include Corey-Bakshi-Shibata reduction, oxidative phenolic cyclization, intramolecular [2+2] photocycloaddition, and intramolecular radical cyclization-benzylic oxidative cyclization, enabling efficient access to 4/5/6/6/6 and 5/5/6/6/6-fused pentacyclic frameworks of these natural products.