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Revisiting Nanoscale Microstructural Features of Alloy 680 to Understand Its Remarkable Mechanical Strength in the As-Welded Condition

  • Cleiton C. Silva,
  • Rafaella S. Silva,
  • Émerson M. Miná,
  • Giovani Dalpiaz,
  • Ricardo R. Marinho,
  • Marcelo T. P. Paes,
  • Marcelo F. Motta,
  • Hélio C. de Miranda,
  • Irina Wossack,
  • Alisson Kwiatkowski da Silva,
  • Christian H. Liebscher

摘要

The present study assesses the microstructureMicrostructure of a new Ni-based alloyNickel-based alloys filler metal, Inconel® 680, at high resolution to understand the underlying mechanisms behind its remarkable mechanical propertiesMechanical properties. Investigations using aberration-corrected (scanning) transmission electron microscopyTransmission electron microscopy (TEM/STEM) were performed to complement the previous microstructural analysis. The results from TEM analysis confirmed Nb-rich C14-type Laves phase precipitationPrecipitation, besides different types of carbides in the interdendritic spacings. However, the advanced microstructural characterisationCharacterisation has also shown a heterogeneous pattern in terms of microstructureMicrostructure between the cellular-dendrite core and interdendritic region. A higher dislocation density was noticed in the interdendritic spacings accompanied by nanometric precipitationPrecipitation. These nanoprecipitates were identified as being tined globular-shape γ″-Ni3Nb phase. The γ″-Ni3Nb phase precipitationPrecipitation resulted from an intense microsegregation of Nb during the solidificationSolidification. This precipitationPrecipitation of the γ″-Ni3Nb phase plays an essential role in the enhanced yield strength ofAlloy 680 alloy 680.