<p>Cu<sub>2</sub>O–ZnO oxide matrix were successfully synthesized by the hydrothermal method. The structural properties, morphology, crystallite and particle size were analyzed using X-Ray Diffraction, Scanning Electron Microscopy, Transmission Electron Microscopy, and Energy-Dispersive X-Ray Spectroscopy techniques. The effect of NaBH<sub>4</sub> and Na<sub>3</sub>C<sub>6</sub>H<sub>5</sub>O<sub>7</sub> as reducing agents was evaluated through Cyclic Voltammetry, Chronoamperometry and Tafel techniques in a 0.1&#xa0;M KHCO<sub>3</sub> supporting electrolyte.</p> Graphical abstract <p></p>

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Cu2O–ZnO oxide matrix synthesized by the hydrothermal method

  • Miguel Ángel Soto-Mendoza,
  • Cindy Xanath Tirado-López,
  • Arturo Manzo-Robledo,
  • Araceli Ezeta-Mejía,
  • Ricardo Gerardo Sánchez-Alvarado

摘要

Cu2O–ZnO oxide matrix were successfully synthesized by the hydrothermal method. The structural properties, morphology, crystallite and particle size were analyzed using X-Ray Diffraction, Scanning Electron Microscopy, Transmission Electron Microscopy, and Energy-Dispersive X-Ray Spectroscopy techniques. The effect of NaBH4 and Na3C6H5O7 as reducing agents was evaluated through Cyclic Voltammetry, Chronoamperometry and Tafel techniques in a 0.1 M KHCO3 supporting electrolyte.

Graphical abstract