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Synthesis of spinel ferrites from cashew gum for microwave devices application

  • Evanimek B. Sabino da Silva,
  • Amanda G. Barboza,
  • Marina de O. Alencar,
  • Crislane P. Nacimento da Silva,
  • M. T. De Melo

摘要

An eco-friendly sol–gel method was used to synthesize spinel nanoparticles (NPs) MxFeyO4, with M being cobalt (Co) or nickel (Ni), and the molar ratio of y/x varying between 1 and 2. These nanoparticles were intended for electromagnetic sensors. Characterization with X-ray diffraction (XRD) with Rietveld refinements and transmission electron microscopy (TEM) with small-angle electron diffraction confirmed that all samples are single phase with a spinel structure and crystallite sizes ranging from 38.5 to 69.3 nm. Coplanar microwave sensors using these NPs involved vector analysis for measuring S-parameters.

Graphical abstract