Abstract <p>Composite electrochemical coatings (CECs) based on nickel and Ti<sub>3</sub>C<sub>2</sub>T<sub><i>x</i></sub> MXene were obtained from a sulfate-chloride electrolyte in galvanostatic mode. Microstructure of these CECs) was studied using X-ray phase analysis and scanning electron microscopy. It was found that the microhardness of nickel–Ti<sub>3</sub>C<sub>2</sub>T<sub><i>x</i></sub> CECs increases by approximately 1.80 times compared to pure nickel. The corrosion-electrochemical behavior of nickel–Ti<sub>3</sub>C<sub>2</sub>T<sub><i>x</i></sub> composite coatings in 0.5 M H<sub>2</sub>SO<sub>4</sub> was studied. Based on tests in 3.5% NaCl, it was found that the inclusion of Ti<sub>3</sub>C<sub>2</sub>T<sub><i>x</i></sub> MXene particles in the electrolytic nickel matrix leads to a decrease in the corrosion rate by 1.60–1.75 times.</p>

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Electrochemical Deposition and Properties of Composite Nickel Coatings Modified with Ti3C2Tx

  • V. N. Tseluikin,
  • A. S. Dzhumieva,
  • A. I. Tribis,
  • D. A. Tikhonov

摘要

Abstract

Composite electrochemical coatings (CECs) based on nickel and Ti3C2Tx MXene were obtained from a sulfate-chloride electrolyte in galvanostatic mode. Microstructure of these CECs) was studied using X-ray phase analysis and scanning electron microscopy. It was found that the microhardness of nickel–Ti3C2Tx CECs increases by approximately 1.80 times compared to pure nickel. The corrosion-electrochemical behavior of nickel–Ti3C2Tx composite coatings in 0.5 M H2SO4 was studied. Based on tests in 3.5% NaCl, it was found that the inclusion of Ti3C2Tx MXene particles in the electrolytic nickel matrix leads to a decrease in the corrosion rate by 1.60–1.75 times.