错误:搜索内容不能为空,请输入英文关键词
错误:关键词超出字数限制,请精简
高级检索

A Quantum-Chemical Study of the Structure of the Complex of Dibenzo-18-Crown-6 Ether with CaCl2 and Its Reactivity in the Oxidation of Ethylbenzene

  • I. S. Rodionov,
  • V. I. Anisimova,
  • N. V. Ulitin,
  • A. A. Baldinov,
  • I. A. Suvorova,
  • N. M. Nurullina,
  • D. A. Shiyan,
  • K. A. Tereshchenko,
  • S N. Tuntseva,
  • T. L. Puchkova,
  • Kh. E. Kharlampidi,
  • O. V. Stoyanov

摘要

Abstract

Ethylbenzene hydroperoxide (EBOOH) is used as an initiator of polymerization of anaerobic adhesives. It was experimentally established that the complex of dibenzo-18-crown-6 ether with CaCl2 (Ca2+∙DBC) accelerates the ethylbenzene oxidation. Based on quantum-chemical modeling by the PBEPBE-GD3/def2TZVP method, it was revealed that the formation of the catalyst’s intermediate adducts with the reaction system’s components is possible and energetically favorable. The O–O bond strength decreases both in α-EBOOH and in β-EBOOH in the adduct EBOOH∙Ca2+∙DBC. However, the adduct α-EBOOH∙Ca2+∙DBC promotes a more rapid decomposition of ethylbenzene hydroperoxide into radicals.