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Regularities of Single-Step Synthesis of Adamantane-Containing Polyimides in Sulfolane

  • A. M. Pichugin,
  • E. M. Sukhareva,
  • A. D. Dubinina,
  • Yu. M. Mkrtchyan,
  • A. A. Panov,
  • E. A. Alykova,
  • E. N. Savel’ev,
  • V. M. Svetlichnyi,
  • I. A. Novakov

摘要

Abstract

It has been shown that adamantane-containing diamines are highly reactive under conditions of single-stage high-temperature cyclization in a sulfolane–toluene mixture of solvents. Polyimides with the reduced viscosity of 1.3‒1.4 dL/g have been synthesized on their bases, the films of which have exhibited good thermal properties and low yellowness index (1.1‒1.2).