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Abstract <p>Acetoacetanilide acetylhydrazone has been synthesized for the first time by the condensation of acetoacetanilide with acetylhydrazide in ethanol. Its structure has been confirmed by elemental analysis, IR and UV spectra, and X-ray analysis. Thermal properties and stability of the title compound have been studied. Acetoacetanilide acetylhydrazone crystallizes in space group <i>P1</i> of the triclinic crystal system, and its stable crystal packing is determined by a system of intermolecular hydrogen bonds and possible π-stacking interactions. The obtain results suggest that compounds structurally related to acetoacetanilide acetylhydrazone are promising as ligands in coordination chemistry.</p>

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Synthesis, Structure, and Properties of Acetoacetanilide Acetylhydrazone

  • 期刊论文

  • 发表日期：

    2025年9月1日

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  • S. Z. Sattorova,
  • H. S. Aminova,
  • S. F. Abdurakhmonov,
  • E. A. Khudoyarova,
  • B. B. Umarov,
  • Z. A. Sulaymonova

摘要

Abstract

Acetoacetanilide acetylhydrazone has been synthesized for the first time by the condensation of acetoacetanilide with acetylhydrazide in ethanol. Its structure has been confirmed by elemental analysis, IR and UV spectra, and X-ray analysis. Thermal properties and stability of the title compound have been studied. Acetoacetanilide acetylhydrazone crystallizes in space group P1 of the triclinic crystal system, and its stable crystal packing is determined by a system of intermolecular hydrogen bonds and possible π-stacking interactions. The obtain results suggest that compounds structurally related to acetoacetanilide acetylhydrazone are promising as ligands in coordination chemistry.