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Chemical Transformations of Fatty Acids in the Hydrolysis of Triglycerides. Selective Isolation of Oleic Acid from Rapeseed Oil under Sub- and Supercritical Water Conditions

  • A. U. Aetov,
  • R. A. Usmanov,
  • R. R. Gabitov,
  • S. V. Mazanov,
  • V. B. Vol’eva,
  • A. V. Ryzhakova,
  • R. Z. Musin,
  • F. M. Gumerov,
  • S. D. Varfolomeev

摘要

Abstract

The hydrolysis of rapeseed oil in sub- and supercritical water (T = 573–653 K, p = 30 MPa) has been studied using a batch setup. Unlike traditional hydrolysis, the hydrothermal process involves in situ change of the fatty acid composition as a result of the transformation of linoleic acid to oleic acid, and there is the possibility of selective isolation of the latter with a purity sufficient for its use for technical purposes without special purification. A stepwise mechanism of the hydrothermal process has been proposed on the basis of analysis of transformation products of individual linoleic acid.