Scholarlink

Abstract <p>The reaction of thioacetamide, cyanothioacetamide, thiourea, 3-aryl-2-cyanothioacrylamides, (cyclohexylidene)cyanothioacetamide, or thiosemicarbazide with <i>N</i>-aryl-2-chloroacetamides in the presence of KOH in ethanol proceeds with the formation of the same products―2,2′-thiobis(<i>N</i>-arylacetamides)―in 62–93% yields. Structure of the products was confirmed by IR, NMR spectroscopy, and high-resolution mass spectrometry (HRMS).</p>

错误：搜索内容不能为空，请输入英文关键词
错误：关键词超出字数限制，请精简
高级检索

Synthesis of 2,2′-Thiobis(N-arylacetamides) by Reaction of Primary Thioamides with N-Aryl-2-chloroacetamides

  • 期刊论文

  • 发表日期：

    2025年9月1日

查看全文
  • V. V. Dotsenko,
  • A. Z. Temerdashev,
  • N. A. Aksenov,
  • I. V. Aksenova,
  • B. S. Krivokolysko,
  • S. G. Krivokolysko

摘要

Abstract

The reaction of thioacetamide, cyanothioacetamide, thiourea, 3-aryl-2-cyanothioacrylamides, (cyclohexylidene)cyanothioacetamide, or thiosemicarbazide with N-aryl-2-chloroacetamides in the presence of KOH in ethanol proceeds with the formation of the same products―2,2′-thiobis(N-arylacetamides)―in 62–93% yields. Structure of the products was confirmed by IR, NMR spectroscopy, and high-resolution mass spectrometry (HRMS).