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Selection of Conditions for Alkylation of 3-Amino-1,2,4-triazole

  • E. A. Petukhova,
  • M. V. Dmitriev,
  • E. A. Danilova

摘要

Abstract

In this work the alkylation of 3-amino-1,2,4-triazole with dichloroethane under phase-transfer catalysis conditions was studied. Synthesis conditions were selected. The structure of 1N-(2-chloroethyl)-3-amino-1,2,4-triazole was proven by IR, 1H, 13C and 2D HSQC NMR spectroscopy, gas chromatography-mass spectrometry and X-ray diffraction.