Interaction of C-Alkylsubstituted-1,5,10,14-tetraazacyclooctadeca-4,13-diene with Carboxylic Acid Halides As a New Method for the Synthesis of C- and N-Acyl-2,3,6,7,8,9-hexahydro-1H-1,5-diazonines

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发表日期：

2024年9月1日

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N. A. Anisimova,
V. V. Mikhailov

摘要

Abstract

The reactions of 2,2,4,11,11,13-hexamethyl-1,5,10,14-tetraazacyclooctadeca-4,13-diene with carboxylic acid chlorohydrides produced C- and N-acyl substituted 2,3,6,7,8,9-hexahydro-1H-1,5-diazonines. The structure of the obtained C- and N-acyldiazonines was studied by ¹H and ¹³C NMR spectroscopy using two-dimensional experiments ¹H-¹³C HMQC, HMBC, ¹H-¹H COSY.