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Abstract— <p>Two polymorphic transformations in molecular crystals, specifically glycine and carbamazepine, as well as the dehydration of carbamazepine dihydrate were used as examples, in order to investigate the effect of jar material (stainless steel versus various polymers) on the outcomes of mechanochemical treatment in vibrational ball mills. The study illustrates, how an in-house accessible method of 3D printing polymer inserts for stainless steel jars can be used to explore these effects.</p>

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Variation of Polymeric Material of Mechanoreactor Walls As a Tool for Influencing Mechanochemical Transformations Involving Molecular Crystals

  • 期刊论文

  • 发表日期：

    2025年5月27日

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  • E. A. Losev,
  • D. Ya. Zheltikova,
  • D. S. Kolybalov,
  • A. G. Ogienko,
  • E. V. Boldyreva

摘要

Abstract—

Two polymorphic transformations in molecular crystals, specifically glycine and carbamazepine, as well as the dehydration of carbamazepine dihydrate were used as examples, in order to investigate the effect of jar material (stainless steel versus various polymers) on the outcomes of mechanochemical treatment in vibrational ball mills. The study illustrates, how an in-house accessible method of 3D printing polymer inserts for stainless steel jars can be used to explore these effects.