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Yttrium(III) Complexes with Carbamide and Dimethylacetamide: Composition, Structure, and Thermal Decomposition

  • E. K. Bettels,
  • M. S. Polukhin,
  • I. A. Karavaev,
  • E. V. Savinkina,
  • G. A. Buzanov,
  • A. S. Kubasov,
  • V. M. Retivov

摘要

Abstract

Yttrium(III) complexes with carbamide (Ur) and N,N-dimethylacetamide (DMAA) of composition [Y(H2O)(Ur)2(NO3)3] (I), [Y(Ur)3(NO3)3] (II), and [Y(DMAA)3(NO3)3] (III) have been synthesized. Their composition, structural features, and thermolysis processes in a wide temperature range have been determined using physicochemical methods (elemental analysis, IR spectroscopy, X-ray powder diffraction, single-crystal X-ray diffraction, thermogravimetric analysis, and differential scanning calorimetry). It has been shown that the isolated complexes can be used for the synthesis of nanosized yttrium oxide.