Scholarlink

<p>This study used the co-precipitation method to produce novel nanorods from bi-functional Co-Ag metal-organic frameworks (BF Co-Ag MOF). CuO was then immobilized onto the BF Co-Ag MOF to create a new heterogeneous catalytic material (BF Co-Ag MOF@CuO). This material was thoroughly examined using several analytical methods, including field-emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDX), transmission electron microscopy (TEM), X-ray diffraction (XRD), N<sub>2</sub> adsorption-desorption, vibrating-sample magnetometry (VSM), and Fourier transform infrared spectroscopy (FT-IR). The one-pot, multi-component Hantzsch fabrication of biologically significant fused 1,4-dihydropyridines (1,4-DHPs) was used to assess the synthesized nanorods’ catalytic efficiency. Dimedone, commercially available aldehydes, and ammonium acetate as a nitrogen source were used in this chemical reaction at 60&#xa0;°C in aqueous media. <sup>1</sup>H-NMR and<sup>13</sup>&#xa0;C-NMR spectroscopy were used to thoroughly analyze the obtained products. The quick fabrication of a wide variety of 1,4-DHPs with short chemical transformation times, straightforward experimental and work-up processes, simple catalytic material preparation, outstanding catalytic performance, notable product outputs, an eco-friendly solvent, and reusability are just a few benefits of the suggested approach.</p>

错误：搜索内容不能为空，请输入英文关键词
错误：关键词超出字数限制，请精简
高级检索

Synthesis and characterization of bi-functional Co-Ag MOF@CuO nanorods as an innovative robust heterogeneous catalytic material for the fabrication of fused 1,4-dihydropyridine derivatives

  • 期刊论文

  • 出版模式：

    开放获取

  • 发表日期：

    2026年5月18日

查看全文
  • Negar Hoot,
  • Enayatollah Sheikhhosseini,
  • Sayed Ali Ahmadi,
  • Mahdieh Yahyazadehfar

摘要

This study used the co-precipitation method to produce novel nanorods from bi-functional Co-Ag metal-organic frameworks (BF Co-Ag MOF). CuO was then immobilized onto the BF Co-Ag MOF to create a new heterogeneous catalytic material (BF Co-Ag MOF@CuO). This material was thoroughly examined using several analytical methods, including field-emission scanning electron microscopy (FE-SEM), energy-dispersive X-ray spectroscopy (EDX), transmission electron microscopy (TEM), X-ray diffraction (XRD), N2 adsorption-desorption, vibrating-sample magnetometry (VSM), and Fourier transform infrared spectroscopy (FT-IR). The one-pot, multi-component Hantzsch fabrication of biologically significant fused 1,4-dihydropyridines (1,4-DHPs) was used to assess the synthesized nanorods’ catalytic efficiency. Dimedone, commercially available aldehydes, and ammonium acetate as a nitrogen source were used in this chemical reaction at 60 °C in aqueous media. 1H-NMR and13 C-NMR spectroscopy were used to thoroughly analyze the obtained products. The quick fabrication of a wide variety of 1,4-DHPs with short chemical transformation times, straightforward experimental and work-up processes, simple catalytic material preparation, outstanding catalytic performance, notable product outputs, an eco-friendly solvent, and reusability are just a few benefits of the suggested approach.