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<p>Glucose sensing remains a crucial need as diabetes is a worldwide concern. This work reports the application of Nb<sub>2</sub>CT<sub><i>x</i></sub>—selenium nanoparticle composite material for the nonenzymatic sensing of glucose. The surface morphology of the synthesized composite was analyzed using various microscopic techniques like scanning electron microscopy, transmission electron microscopy, and its structural properties were analyzed using diffraction and spectroscopic methods. A gold disc electrode was modified using the nanocomposite and tested for glucose in an alkaline medium. The sensing was based on the oxidation of glucose on the catalytic surface. The glucose was quantified amperometrically at a significantly lower overpotential of 0.16&#xa0;V. The sensor showed a good detection range from 2 to 30&#xa0;mM with a sensitivity of 4.15&#xa0;µA mM<sup>−1</sup>&#xa0;cm<sup>−2</sup> and a detection limit of 1.1&#xa0;mM.</p>

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Selenium nanoparticles modified niobium MXene for non-enzymatic detection of glucose

  • 期刊论文

  • 出版模式：

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  • 发表日期：

    2025年1月11日

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  • Prabisha K. E.,
  • Neena P. K.,
  • Menon Ankitha,
  • P. Abdul Rasheed,
  • P. V. Suneesh,
  • T. G. Satheesh Babu

摘要

Glucose sensing remains a crucial need as diabetes is a worldwide concern. This work reports the application of Nb2CTx—selenium nanoparticle composite material for the nonenzymatic sensing of glucose. The surface morphology of the synthesized composite was analyzed using various microscopic techniques like scanning electron microscopy, transmission electron microscopy, and its structural properties were analyzed using diffraction and spectroscopic methods. A gold disc electrode was modified using the nanocomposite and tested for glucose in an alkaline medium. The sensing was based on the oxidation of glucose on the catalytic surface. The glucose was quantified amperometrically at a significantly lower overpotential of 0.16 V. The sensor showed a good detection range from 2 to 30 mM with a sensitivity of 4.15 µA mM−1 cm−2 and a detection limit of 1.1 mM.