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Physical and structural characterization of bis-acryl composite resin

  • Wendy E. Rodríguez-Guardado,
  • Eric M. Rivera-Muñoz,
  • Janeth Serrano-Bello,
  • Marco A. Alvarez-Perez,
  • Rubén A. Domínguez-Pérez,
  • Elias Nahum Salmerón-Valdés,
  • Febe C. Vázquez Vázquez,
  • Osmar A. Chanes-Cuevas,
  • Beatriz Millán-Malo,
  • Carmen L. Peza-Ledesma,
  • Rodrigo Correa-Prado

摘要

During the preparation of fixed prosthesis (including individual bridges and crowns) it is important to select the materials that have the best features and properties to predict a successful clinical treatment. The objective of this study was to determine if the chemical and structural characteristics could cause to increase the fracture resistance, we used four bis-acryl resins Luxatemp, Protemp, Structur and Telio. Three-points bending by Flexural test were performed in ten bars and they were carried out to compare with Anova test. In addition, the bis-acryl resins were analyzed by scanning electron microscopy, to analyze microstructure and morphology and the molecular structure were performed by Infrared Spectroscopy through Attenuated Total Reflectance. A higher flexural strength was found in Luxatemp and Structur with, no significant differences between this study groups. Regarding Protemp and Telio, these study groups showed a lower flexural strength when were compared with Luxatemp and Structur. These results corroborate SEM and ATR analysis because Luxatemp sample showed a regular size particle on the surface and chemically presents a long cross-linkage polymer chain. The presence of CO3, SiO2 and N–H groups as a fillers particle interacting with OH groups cause a higher flexural strength compared with another groups.