<p>The construction of artificial light-harvesting systems (LHSs) with continuous chirality transfer is of great significance to deeply comprehend the hierarchical evolution in nature. Herein, the achiral C<sub>3</sub>-symmetric benzene-1,3,5-tricarboxamide (BTA) molecule functions as donor of LHSs motifs, where subnanometer-scale metal clusters (<i>R</i>/<i>S</i>-Ag<sub>6</sub>) are introduced as “Sergeants” to generate predominant handedness nanoribbons through chirality transfer. Importantly, these helical nanoribbons act as chirality and energy donors for the energy level-matching Ag<sub>6</sub>-cluster acceptors, enabling the fabrication of chirality-controlled LHSs that achieve amplified circularly polarized luminescence (CPL) of Ag<sub>6</sub> clusters with a dissymmetry factor (|<i>g</i><sub>lum</sub>|) of 1 × 10<sup>-2</sup>. Notably, the CPL signals of <i>R</i>/<i>S</i>-Ag<sub>6</sub> are further distinctly amplified with |<i>g</i><sub>lum</sub>| reaching 6 × 10<sup>-2</sup> through chirality-matching and synergistic effect of <i>R</i>/<i>S</i>-1-phenylethanol. Furthermore, <i>R</i>/<i>S</i>-Cu<sub>6</sub> clusters with near-infrared emission are employed as the second acceptor to construct relayed homochiral LHSs. Such LHSs program continuous chirality and energy transfers from BTA assemblies to Ag<sub>6</sub> and then to Ag<sub>x</sub>Cu<sub>6-x</sub> alloy clusters, ultimately resulting in near-infrared CPL with |<i>g</i><sub>lum</sub>| of 5 × 10<sup>-2</sup>. This work provides valuable insight into the mechanisms of CPL transmission and amplification in cluster-driven chiral LHSs and opens potential application in chiroptical encryption.</p>

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Chiral metal cluster-mediated chirality transfer in light-harvesting nanoribbons for amplified circularly polarized luminescence

  • Tian-Li Gao,
  • Jun-Ru Wang,
  • Zhen Han,
  • Jia-Yin Wang,
  • Ying-Xue Yuan,
  • Shuang-Quan Zang

摘要

The construction of artificial light-harvesting systems (LHSs) with continuous chirality transfer is of great significance to deeply comprehend the hierarchical evolution in nature. Herein, the achiral C3-symmetric benzene-1,3,5-tricarboxamide (BTA) molecule functions as donor of LHSs motifs, where subnanometer-scale metal clusters (R/S-Ag6) are introduced as “Sergeants” to generate predominant handedness nanoribbons through chirality transfer. Importantly, these helical nanoribbons act as chirality and energy donors for the energy level-matching Ag6-cluster acceptors, enabling the fabrication of chirality-controlled LHSs that achieve amplified circularly polarized luminescence (CPL) of Ag6 clusters with a dissymmetry factor (|glum|) of 1 × 10-2. Notably, the CPL signals of R/S-Ag6 are further distinctly amplified with |glum| reaching 6 × 10-2 through chirality-matching and synergistic effect of R/S-1-phenylethanol. Furthermore, R/S-Cu6 clusters with near-infrared emission are employed as the second acceptor to construct relayed homochiral LHSs. Such LHSs program continuous chirality and energy transfers from BTA assemblies to Ag6 and then to AgxCu6-x alloy clusters, ultimately resulting in near-infrared CPL with |glum| of 5 × 10-2. This work provides valuable insight into the mechanisms of CPL transmission and amplification in cluster-driven chiral LHSs and opens potential application in chiroptical encryption.