<p>This paper describes the design and performance of the tender energy spectroscopy beamline (BL16U1), a phase II beamline, at the Shanghai Synchrotron Radiation Facility. The beamline, based on an in-vacuum undulator source with 26&#xa0;mm period, provides an operable energy range between 2.1 keV and 16 keV, covering the K-edges of P to Rb and <InlineEquation ID="IEq1"> <EquationSource Format="TEX">\(\mathrm L_{3}\)</EquationSource> <EquationSource Format="MATHML"><math> <msub> <mi mathvariant="normal">L</mi> <mn>3</mn> </msub> </math></EquationSource> </InlineEquation>-edges of Zr to Bi. The principal optical elements of the beamline are a toroidal mirror, a liquid nitrogen-cooled double-crystal monochromator, a high-harmonic-rejection mirror, and two pairs of Kirkpatrick–Baez (KB) mirrors. Three end-stations, including non-focusing, microprobe, and sub-microprobe types, are installed on the beamline. X-ray fluorescence (XRF) and X-ray absorption spectroscopy (XAS), including X-ray absorption near-edge structure (XANES) and extended X-ray absorption fine structure (EXAFS), are performed under vacuum or He atmosphere at the non-focusing end-station (with a beam spot size of <InlineEquation ID="IEq2"> <EquationSource Format="TEX">\(\sim {670}\,{\upmu \hbox {m}}\times {710}\,{\upmu \hbox {m}}\)</EquationSource> <EquationSource Format="MATHML"><math> <mrow> <mo>∼</mo> <mn>670</mn> <mspace width="0.166667em" /> <mrow> <mi mathvariant="normal">μ</mi> <mtext>m</mtext> </mrow> <mo>×</mo> <mn>710</mn> <mspace width="0.166667em" /> <mrow> <mi mathvariant="normal">μ</mi> <mtext>m</mtext> </mrow> </mrow> </math></EquationSource> </InlineEquation>). Using two KB mirrors systems, micro-XRF (<InlineEquation ID="IEq3"> <EquationSource Format="TEX">\(\upmu\)</EquationSource> <EquationSource Format="MATHML"><math> <mi mathvariant="normal">μ</mi> </math></EquationSource> </InlineEquation>XRF) mapping and micro-XANES (<InlineEquation ID="IEq4"> <EquationSource Format="TEX">\(\upmu\)</EquationSource> <EquationSource Format="MATHML"><math> <mi mathvariant="normal">μ</mi> </math></EquationSource> </InlineEquation>XANES) studies can be performed with a spot size of approximately <InlineEquation ID="IEq5"> <EquationSource Format="TEX">\(\sim {3.3}\,{\upmu \hbox {m}}\times {1.3}\,{\upmu \hbox {m}}\)</EquationSource> <EquationSource Format="MATHML"><math> <mrow> <mo>∼</mo> <mrow> <mn>3.3</mn> </mrow> <mspace width="0.166667em" /> <mrow> <mi mathvariant="normal">μ</mi> <mtext>m</mtext> </mrow> <mo>×</mo> <mrow> <mn>1.3</mn> </mrow> <mspace width="0.166667em" /> <mrow> <mi mathvariant="normal">μ</mi> <mtext>m</mtext> </mrow> </mrow> </math></EquationSource> </InlineEquation> at the microprobe end-station and with a smaller spot size of <InlineEquation ID="IEq6"> <EquationSource Format="TEX">\(\sim {0.5}\,{\upmu \hbox {m}}\times {0.25}\,{\upmu \hbox {m}}\)</EquationSource> <EquationSource Format="MATHML"><math> <mrow> <mo>∼</mo> <mrow> <mn>0.5</mn> </mrow> <mspace width="0.166667em" /> <mrow> <mi mathvariant="normal">μ</mi> <mtext>m</mtext> </mrow> <mo>×</mo> <mrow> <mn>0.25</mn> </mrow> <mspace width="0.166667em" /> <mrow> <mi mathvariant="normal">μ</mi> <mtext>m</mtext> </mrow> </mrow> </math></EquationSource> </InlineEquation> at the sub-microprobe end-station. The non-focusing end-station was officially opened to users in January 2024. The microprobe and sub-microprobe end-stations will be opened to users in the near future. This paper presents the characteristics, short-term technical developments, and early experimental results of this new beamline.</p>

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Tender energy spectroscopy beamline at the Shanghai Synchrotron Radiation Facility

  • Shu-Min Yang,
  • Ling-Ling Guo,
  • Bing Nan,
  • Ying Zhao,
  • Yan-Qing Wu,
  • Zhi Guo,
  • Chen Tian,
  • Bo Zhao,
  • Chao-Fan Xue,
  • Jun Zhao,
  • Shuang Song,
  • Zhen-Ye Liang,
  • Li-Na Li,
  • Yong Wang,
  • Ren-Zhong Tai

摘要

This paper describes the design and performance of the tender energy spectroscopy beamline (BL16U1), a phase II beamline, at the Shanghai Synchrotron Radiation Facility. The beamline, based on an in-vacuum undulator source with 26 mm period, provides an operable energy range between 2.1 keV and 16 keV, covering the K-edges of P to Rb and \(\mathrm L_{3}\) L 3 -edges of Zr to Bi. The principal optical elements of the beamline are a toroidal mirror, a liquid nitrogen-cooled double-crystal monochromator, a high-harmonic-rejection mirror, and two pairs of Kirkpatrick–Baez (KB) mirrors. Three end-stations, including non-focusing, microprobe, and sub-microprobe types, are installed on the beamline. X-ray fluorescence (XRF) and X-ray absorption spectroscopy (XAS), including X-ray absorption near-edge structure (XANES) and extended X-ray absorption fine structure (EXAFS), are performed under vacuum or He atmosphere at the non-focusing end-station (with a beam spot size of \(\sim {670}\,{\upmu \hbox {m}}\times {710}\,{\upmu \hbox {m}}\) 670 μ m × 710 μ m ). Using two KB mirrors systems, micro-XRF ( \(\upmu\) μ XRF) mapping and micro-XANES ( \(\upmu\) μ XANES) studies can be performed with a spot size of approximately \(\sim {3.3}\,{\upmu \hbox {m}}\times {1.3}\,{\upmu \hbox {m}}\) 3.3 μ m × 1.3 μ m at the microprobe end-station and with a smaller spot size of \(\sim {0.5}\,{\upmu \hbox {m}}\times {0.25}\,{\upmu \hbox {m}}\) 0.5 μ m × 0.25 μ m at the sub-microprobe end-station. The non-focusing end-station was officially opened to users in January 2024. The microprobe and sub-microprobe end-stations will be opened to users in the near future. This paper presents the characteristics, short-term technical developments, and early experimental results of this new beamline.