<p>With the rapid development of nuclear energy, the removal of radioactive iodine generated during spent fuel reprocessing has become increasingly important. Based on the unique straw-like structure of populus tomentosa fiber (PTF) and the highly active iodine vapor capture ability of zero-valent silver nanoparticles (PTF@Ag<sup>0</sup>NP), an Ag<sup>0</sup>NP composite functional material with highly efficient iodine vapor capture capability was synthesized from biowaste PTF through ultrasonic and high-temperature hydrothermal methods in this study. The iodine capture experiment demonstrated that PTF@Ag<sup>0</sup>NP exhibits rapid iodine capture efficiency, reaching dynamic equilibrium within 4&#xa0;h and a maximum capture capacity of 1008.1&#xa0;mg/g. Density functional theory calculations show that PTF@Ag<sup>0</sup>NP exhibits extremely high chemical reactivity toward iodine, with a reaction binding energy of <InlineEquation ID="IEq1"> <InlineMediaObject> <ImageObject Color="BlackWhite" FileRef="41365_2025_1647_Article_IEq1.gif" Format="GIF" Height="13" Rendition="HTML" Resolution="72" Type="Linedraw" Width="19" /> </InlineMediaObject> <EquationSource Format="TEX">\(-\)</EquationSource> <EquationSource Format="MATHML"><math> <mo>-</mo> </math></EquationSource> </InlineEquation>2.88&#xa0;eV. Additionally, the molecular dynamics of PTF@Ag<sup>0</sup>NP indicate that there is no atomic displacement at 77&#xa0;<InlineEquation ID="IEq2"> <InlineMediaObject> <ImageObject Color="BlackWhite" FileRef="41365_2025_1647_Article_IEq2.gif" Format="GIF" Height="14" Rendition="HTML" Resolution="72" Type="Linedraw" Width="20" /> </InlineMediaObject> <EquationSource Format="TEX">\(^{\circ }\text {C}\)</EquationSource> <EquationSource Format="MATHML"><math> <mrow> <mmultiscripts> <mrow /> <mrow /> <mo>∘</mo> </mmultiscripts> <mtext>C</mtext> </mrow> </math></EquationSource> </InlineEquation>, indicating the excellent temperature stability of the material at the operating temperature. The capture mechanism suggests that iodine vapor primarily reacts with Ag<sup>0</sup>NP to form AgI, and that the hydroxyl groups in PTF can also effectively capture iodine vapor by adsorption induction. In conclusion, PTF@Ag<sup>0</sup>NP is expected to be an effective candidate adsorbent material for removing radioactive iodine vapor from exhaust gases during spent fuel reprocessing.</p>

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Zero-valent silver nanoparticles functionalized populus tomentosa fiber for efficient capture and immobilization of iodine vapor

  • Yu Fang,
  • Hui Zhu,
  • Pei Chen,
  • Fang Liu,
  • Yong Yi,
  • Jian Zhou,
  • Tao Duan,
  • Jie-Hong Lei

摘要

With the rapid development of nuclear energy, the removal of radioactive iodine generated during spent fuel reprocessing has become increasingly important. Based on the unique straw-like structure of populus tomentosa fiber (PTF) and the highly active iodine vapor capture ability of zero-valent silver nanoparticles (PTF@Ag0NP), an Ag0NP composite functional material with highly efficient iodine vapor capture capability was synthesized from biowaste PTF through ultrasonic and high-temperature hydrothermal methods in this study. The iodine capture experiment demonstrated that PTF@Ag0NP exhibits rapid iodine capture efficiency, reaching dynamic equilibrium within 4 h and a maximum capture capacity of 1008.1 mg/g. Density functional theory calculations show that PTF@Ag0NP exhibits extremely high chemical reactivity toward iodine, with a reaction binding energy of \(-\) - 2.88 eV. Additionally, the molecular dynamics of PTF@Ag0NP indicate that there is no atomic displacement at 77  \(^{\circ }\text {C}\) C , indicating the excellent temperature stability of the material at the operating temperature. The capture mechanism suggests that iodine vapor primarily reacts with Ag0NP to form AgI, and that the hydroxyl groups in PTF can also effectively capture iodine vapor by adsorption induction. In conclusion, PTF@Ag0NP is expected to be an effective candidate adsorbent material for removing radioactive iodine vapor from exhaust gases during spent fuel reprocessing.