Scholarlink

<p>Three-component reaction between arylglyoxals, barbituric/thiobarbituric acid and ammonium/potassium thiocyanate led to the synthesis of ammonium barbiturate/thiobarbiturate and potassium barbiturate derivatives in high yields. All reactions were carried out in ethanol as a safe solvent without the use of a catalyst. The stable solid products were easily isolated and purified by washing with water and ethanol without the need for chromatographic methods. The structures of the products were confirmed by <sup>1</sup>H, <sup>13</sup>C-NMR, IR, and elemental analysis.</p>

错误：搜索内容不能为空，请输入英文关键词
错误：关键词超出字数限制，请精简
高级检索

An efficient synthesis of new barbiturate/thiobarbiturate salts by the reaction between arylglyoxals, barbituric/thiobarbituric acid and ammonium/potassium thiocyanate

  • 期刊论文

  • 发表日期：

    2026年1月5日

查看全文
  • Maryam Oudi,
  • Mohammad Anary-Abbasinejad

摘要

Three-component reaction between arylglyoxals, barbituric/thiobarbituric acid and ammonium/potassium thiocyanate led to the synthesis of ammonium barbiturate/thiobarbiturate and potassium barbiturate derivatives in high yields. All reactions were carried out in ethanol as a safe solvent without the use of a catalyst. The stable solid products were easily isolated and purified by washing with water and ethanol without the need for chromatographic methods. The structures of the products were confirmed by 1H, 13C-NMR, IR, and elemental analysis.