<p>The square wave voltammetry (SWV) method was utilized to simultaneously find paracetamol and p-aminophenol (PAP) by applying an activated glassy carbon electrode (AGCE). The results showed that the AGCE effectively facilitated the oxidation of both compounds, exhibiting a significant separation of their oxidation peaks by approximately 280.5&#xa0;mV, which is sufficient for their concurrent detection. The linear ranges and detection limits were found to be 6.0 × 10<sup>−7</sup>–1.0 × 10<sup>−4</sup>&#xa0;mol L<sup>−1</sup> and 1.0 × 10<sup>−6</sup>–8.0 × 10<sup>−4</sup>&#xa0;mol L<sup>−1</sup>; 1.39 × 10<sup><i>−</i>8</sup>&#xa0;mol L<sup>−1</sup> and 1.91 × 10<sup><i>−</i>8</sup>&#xa0;mol L<sup><i>−</i>1</sup> for APAP and PAP, correspondingly. Ultimately, the adopted method was effectively implemented to measure APAP and PAP in commercial-grade tablets, yielding average recoveries of 103.1% for APAP and 101.0% for PAP.</p> Graphical Abstract <p></p>

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Detection and Separation of Paracetamol and p-Aminophenol Using Activated Glassy Carbon Electrodes

  • Dereje Yenealem,
  • Shimelis Admassie,
  • Santhi Raju Pilli,
  • Sowjanya Motana,
  • Dessie Tibebe

摘要

The square wave voltammetry (SWV) method was utilized to simultaneously find paracetamol and p-aminophenol (PAP) by applying an activated glassy carbon electrode (AGCE). The results showed that the AGCE effectively facilitated the oxidation of both compounds, exhibiting a significant separation of their oxidation peaks by approximately 280.5 mV, which is sufficient for their concurrent detection. The linear ranges and detection limits were found to be 6.0 × 10−7–1.0 × 10−4 mol L−1 and 1.0 × 10−6–8.0 × 10−4 mol L−1; 1.39 × 108 mol L−1 and 1.91 × 108 mol L1 for APAP and PAP, correspondingly. Ultimately, the adopted method was effectively implemented to measure APAP and PAP in commercial-grade tablets, yielding average recoveries of 103.1% for APAP and 101.0% for PAP.

Graphical Abstract