Mechanical and Wear Response of TiO2 Scaffolds Processed via Powder Metallurgy
摘要
In the present work, TiO2 scaffolds are prepared by space holder technique via powder metallurgy. NaCl (0–20 vol%) is used as the space holder material to process TiO2 scaffolds with varied porosity between 13.70 and 35.41%. The calcination of the TiO2 powders resulted improvement in the density and mechanical properties of TiO2 scaffolds after sintering (at 1500 °C for 2 h). The XRD of sintered TiO2 revealed presence of only rutile phase, whereas the starting TiO2 powders possess both anatase and rutile crystalline phases. Depending on the processing conditions, the Young’s modulus and the compression strength of TiO2 measured in the range of 0.68–17.50 GPa and 18.62–360.40 MPa, respectively. A very low COF of 0.104 is evident for TiO2 disk after sliding against Si3N4 ball. Low wear rate of 1.10 × 10–7 mm3/m N was measured for TiO2, and it falls within the mild wear regime. These properties of TiO2 clearly indicate its potential for both the cortical and cancellous bone applications. However, future study needs to be focused on controlling pore morphology of TiO2 scaffolds.