Spark Plasma Sintering of TaC and TaC-SiC Composites: Densification, Microstructure and Electrical Discharge Machinability
摘要
The present study deals with the effect of silicon carbide (SiC) reinforcement on the densification, microstructure, mechanical properties, and electrical discharge machinability of TaC ceramics processed via spark plasma sintering. Two-stage sintering with an optimum sintering temperature of 1900 °C was used to achieve a relative density of ~ 97% for monolithic TaC ceramics, whereas a relative density of > 98% was obtained for TaC—(20 to 65 vol%) SiC powder mixtures with single-stage sintering at 1800 °C. Besides facilitating densification, SiC addition restricted the growth of TaC grains. The hardness of TaC-SiC composites increased with an increase in SiC content, whereas fracture toughness increased beyond 50 vol% SiC addition. Wire-electrical discharge machining (EDM) revealed that TaC–35 vol% SiC composite offered the best combination of machinability (material removal rate of 11.8 mg/min) and surface finish (surface roughness of 1.58 µm). These results highlight the potential of TaC–SiC composites for fabricating critical end, complex-shaped components for advanced strategic structural applications.