<p>Cyclohexane oxidation is crucial in producing adipic acid and caprolactam, essential precursors for the manufacture of various polymers. However, homogeneous catalysts achieve the highest cyclohexane conversion, suggesting the need for further research. We present a facile synthesis of mesoporous tungsten oxide-doped titania (WO₃-TiO₂) supported on the Technische Universitat Delft-Crystalline (TUD-C) material for enhanced cyclohexane photo-oxidation under visible light. In this work, TUD-C mesoporous zeolite was applied as a catalytic support material for WO₃-TiO₂. Various molar percentages of WO₃ (0–1&#xa0;mol%) were doped into TiO₂ to achieve the optimal ratio for maximum catalytic performance. FTIR, XRD, and XPS analyses indicated that Mordenite Framework Inverted (MFI) zeolitic frameworks formed within the TUD-C support materials. Additionally, the porosity study showed that the resulting TUD-C-supported materials were mesoporous and possessed high specific areas. Based on the DRUV-Vis spectra obtained, WO₃ was loaded into TiO₂ in all the TUD-C-supported WO₃-TiO₂ samples, resulting in improved photocatalytic efficiency due to increase in oxidative sites and reduced band gap. FESEM and TEM analysis results revealed uniform dispersion of WO₃-TiO₂ on TUD-C, without agglomeration or aggregation of the particles. The photocatalytic performance of WO₃-doped TiO₂ supported on TUD-C materials was evaluated for cyclohexane photo-oxidation under visible light for 4&#xa0;h. Results demonstrated that TiO₂ photocatalytic activity was enhanced 2-fold in the presence of WO₃ dopant and TUD-C support. These findings strongly suggest that the promising catalysts supported on TUD-C materials can be synthesized via a simple, eco-friendly, and cost-effective approach, potentially enabling large-scale manufacturing of products that meet future clean energy needs.</p>