<p>In this study, a new naphthoquinone derivative molecule was synthesized with a very high yield (99.0%), and its sensor properties were investigated. The characterization of the synthesized molecule was carried out using spectroscopic methods such as <sup>1</sup>H-, <sup>13</sup>C-NMR and FT-IR. Polymer membrane potentiometric sensors were prepared using this molecule as an ionophore, and these newly prepared sensors exhibited selective behavior toward barium(II) ions. The one of barium(II)-selective potentiometric sensors developed had a low detection limit of 3.51 × 10<sup>−6</sup>&#xa0;mol&#xa0;L<sup>−1</sup> in a wide concentration range of 1.0 × 10<sup>−1</sup>–1.0 × 10<sup>−5</sup>&#xa0;mol&#xa0;L<sup>−1</sup> and had also a near-Nernstian behavior. The proposed barium(II) selective sensor was shown to have good reproducibility, fast response time (&lt; 5&#xa0;s), wide pH working range (5.0–10.0) and low cost production. Besides, it could detect barium(II) ions in various water samples with high recoveries; and based on its advantages, it can be proposed as a new alternative in the analysis of barium(II) ions.</p>

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Synthesis, characterization and sensor applications of a new 1,4-naphthoquinone derivative molecule

  • Oguz Özbek,
  • Onur Cem Altunoluk,
  • Kıymet Berkil Akar,
  • Ömer Isildak

摘要

In this study, a new naphthoquinone derivative molecule was synthesized with a very high yield (99.0%), and its sensor properties were investigated. The characterization of the synthesized molecule was carried out using spectroscopic methods such as 1H-, 13C-NMR and FT-IR. Polymer membrane potentiometric sensors were prepared using this molecule as an ionophore, and these newly prepared sensors exhibited selective behavior toward barium(II) ions. The one of barium(II)-selective potentiometric sensors developed had a low detection limit of 3.51 × 10−6 mol L−1 in a wide concentration range of 1.0 × 10−1–1.0 × 10−5 mol L−1 and had also a near-Nernstian behavior. The proposed barium(II) selective sensor was shown to have good reproducibility, fast response time (< 5 s), wide pH working range (5.0–10.0) and low cost production. Besides, it could detect barium(II) ions in various water samples with high recoveries; and based on its advantages, it can be proposed as a new alternative in the analysis of barium(II) ions.