<p>In this work, we successfully enhanced the thermoelectric potential of SbSnO<sub>2</sub> thin films via post-growth annealing. A giant power factor of 51.64 × 10<sup>−4</sup>&#xa0;W&#xa0;m<sup>−1</sup>&#xa0;K<sup>−2</sup> and a moderate figure of merit (ZT) of 0.20 were achieved by annealing Sb-doped SnO<sub>2</sub> thin films at 400°C. Thin films used in this study were synthesized using thermal evaporation followed by post-growth annealing at different temperatures. X-ray diffraction (XRD) data indicated that the as-grown sample has a mixed structure with SnO, SnO<sub>2</sub>, SbO, and SnSb phases, while the sample annealed at 350°C has a pure tetragonal SnO<sub>2</sub> phase, and this phase completely converted into the SbO phase when the annealing temperature reached 400°C. Significant morphological changes were seen in the Sb-doped SnO<sub>2</sub> samples by scanning electron microscopy (SEM), with the sample annealed at 400°C showing a mixed morphology of nanoparticles and nanowires. Electrical conductivity measurements indicate an enhancement in electrical conductivity with increasing annealing temperature, with the maximum value of 105.82 S/cm achieved for the sample annealed at 350°C. The Seebeck coefficient data show a decreasing trend, but annealing at 400°C caused a suddenly increase in the Seebeck coefficient to 105 × 10<sup>−4</sup>&#xa0;V/K, which resulted in a giant power factor value of 51.64 × 10<sup>−4</sup>&#xa0;W&#xa0;m<sup>−1</sup>&#xa0;K<sup>−2</sup><i>.</i> Furthermore, through optimization of the thermal conductivity and power factor, we achieved ZT of 0.20 in the sample annealed at 400°C.</p>

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Achievement of Giant Power Factor and Moderate ZT in Sb-Doped SnO2 Thin Films by Post-Growth Annealing Technique

  • M. Ibrahim,
  • K. Mahmood,
  • A. Ali

摘要

In this work, we successfully enhanced the thermoelectric potential of SbSnO2 thin films via post-growth annealing. A giant power factor of 51.64 × 10−4 W m−1 K−2 and a moderate figure of merit (ZT) of 0.20 were achieved by annealing Sb-doped SnO2 thin films at 400°C. Thin films used in this study were synthesized using thermal evaporation followed by post-growth annealing at different temperatures. X-ray diffraction (XRD) data indicated that the as-grown sample has a mixed structure with SnO, SnO2, SbO, and SnSb phases, while the sample annealed at 350°C has a pure tetragonal SnO2 phase, and this phase completely converted into the SbO phase when the annealing temperature reached 400°C. Significant morphological changes were seen in the Sb-doped SnO2 samples by scanning electron microscopy (SEM), with the sample annealed at 400°C showing a mixed morphology of nanoparticles and nanowires. Electrical conductivity measurements indicate an enhancement in electrical conductivity with increasing annealing temperature, with the maximum value of 105.82 S/cm achieved for the sample annealed at 350°C. The Seebeck coefficient data show a decreasing trend, but annealing at 400°C caused a suddenly increase in the Seebeck coefficient to 105 × 10−4 V/K, which resulted in a giant power factor value of 51.64 × 10−4 W m−1 K−2. Furthermore, through optimization of the thermal conductivity and power factor, we achieved ZT of 0.20 in the sample annealed at 400°C.