<p>Synchrotron monochromatic beam x-ray topography of 4H-SiC epiwafers was conducted in the conventional grazing incidence reflection 11<InlineEquation ID="IEq2"> <InlineMediaObject> <ImageObject Color="BlackWhite" FileRef="11664_2025_11918_Article_IEq2.gif" Format="GIF" Height="16" Rendition="HTML" Resolution="72" Type="Linedraw" Width="10" /> </InlineMediaObject> <EquationSource Format="TEX">\(\overline{2 }\)</EquationSource> <EquationSource Format="MATHML"><math> <mover> <mn>2</mn> <mo>¯</mo> </mover> </math></EquationSource> </InlineEquation>8 at 9&#xa0;keV and also the 2nd order harmonic reflection 22<InlineEquation ID="IEq3"> <InlineMediaObject> <ImageObject Color="BlackWhite" FileRef="11664_2025_11918_Article_IEq3.gif" Format="GIF" Height="16" Rendition="HTML" Resolution="72" Type="Linedraw" Width="10" /> </InlineMediaObject> <EquationSource Format="TEX">\(\overline{4 }\)</EquationSource> <EquationSource Format="MATHML"><math> <mover> <mn>4</mn> <mo>¯</mo> </mover> </math></EquationSource> </InlineEquation> 16 reflection at 18&#xa0;keV. The contrast of defects on the 22<InlineEquation ID="IEq4"> <InlineMediaObject> <ImageObject Color="BlackWhite" FileRef="11664_2025_11918_Article_IEq3.gif" Format="GIF" Height="16" Rendition="HTML" Resolution="72" Type="Linedraw" Width="10" /> </InlineMediaObject> <EquationSource Format="TEX">\(\overline{4 }\)</EquationSource> <EquationSource Format="MATHML"><math> <mover> <mn>4</mn> <mo>¯</mo> </mover> </math></EquationSource> </InlineEquation> 16 reflection is significantly different from that on the 11<InlineEquation ID="IEq5"> <InlineMediaObject> <ImageObject Color="BlackWhite" FileRef="11664_2025_11918_Article_IEq2.gif" Format="GIF" Height="16" Rendition="HTML" Resolution="72" Type="Linedraw" Width="10" /> </InlineMediaObject> <EquationSource Format="TEX">\(\overline{2 }\)</EquationSource> <EquationSource Format="MATHML"><math> <mover> <mn>2</mn> <mo>¯</mo> </mover> </math></EquationSource> </InlineEquation>8 due to the deeper penetration of the x-rays. Further, topographs in 22<InlineEquation ID="IEq6"> <InlineMediaObject> <ImageObject Color="BlackWhite" FileRef="11664_2025_11918_Article_IEq3.gif" Format="GIF" Height="16" Rendition="HTML" Resolution="72" Type="Linedraw" Width="10" /> </InlineMediaObject> <EquationSource Format="TEX">\(\overline{4 }\)</EquationSource> <EquationSource Format="MATHML"><math> <mover> <mn>4</mn> <mo>¯</mo> </mover> </math></EquationSource> </InlineEquation> 16 reflection are characterized by weaker background phase contrast from the beryllium window mounted at the exit of the synchrotron x-ray beam. Ray tracing simulations of contrast of threading edge/screw/mix dislocations, and screw type basal plane dislocations on the 22<InlineEquation ID="IEq7"> <InlineMediaObject> <ImageObject Color="BlackWhite" FileRef="11664_2025_11918_Article_IEq3.gif" Format="GIF" Height="16" Rendition="HTML" Resolution="72" Type="Linedraw" Width="10" /> </InlineMediaObject> <EquationSource Format="TEX">\(\overline{4 }\)</EquationSource> <EquationSource Format="MATHML"><math> <mover> <mn>4</mn> <mo>¯</mo> </mover> </math></EquationSource> </InlineEquation> 16 reflections have been performed and good correlations obtained between the simulations and contrast in topographs.</p>

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Analysis of Dislocation Contrast in Grazing Incidence Synchrotron Monochromatic Beam X-ray Topographs of 4H-SiC Wafers in 22\(\bar{4}\) 16 Reflection

  • Zeyu Chen,
  • Qianyu Cheng,
  • Shanshan Hu,
  • Balaji Raghothamachar,
  • Michael Dudley

摘要

Synchrotron monochromatic beam x-ray topography of 4H-SiC epiwafers was conducted in the conventional grazing incidence reflection 11 \(\overline{2 }\) 2 ¯ 8 at 9 keV and also the 2nd order harmonic reflection 22 \(\overline{4 }\) 4 ¯ 16 reflection at 18 keV. The contrast of defects on the 22 \(\overline{4 }\) 4 ¯ 16 reflection is significantly different from that on the 11 \(\overline{2 }\) 2 ¯ 8 due to the deeper penetration of the x-rays. Further, topographs in 22 \(\overline{4 }\) 4 ¯ 16 reflection are characterized by weaker background phase contrast from the beryllium window mounted at the exit of the synchrotron x-ray beam. Ray tracing simulations of contrast of threading edge/screw/mix dislocations, and screw type basal plane dislocations on the 22 \(\overline{4 }\) 4 ¯ 16 reflections have been performed and good correlations obtained between the simulations and contrast in topographs.