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De novo synthesis of atropisomeric benzofurans via Cu/SPDO complex catalyzed asymmetric formal [3 + 2] annulation

  • Fan-Xiao Meng,
  • Xing-Yu Wang,
  • Ka Lu,
  • Ju-Song Yang,
  • Fu-Min Zhang,
  • Ai-Jun Ma,
  • Bao Du,
  • Yong-Qiang Tu

摘要

Herein, the de novo synthesis of atropisomeric benzofurans through the Cu/spirocyclic-pyrrolidine-oxazoline (SPDO) complex catalyze asymmetric formal [3 + 2] cycloaddition between quinones and ynamides is explored, producing a range of structurally diverse axially chiral benzofurans in satisfactory yields with good to excellent enantioselectivities. Furthermore, density functional theory calculations were applied to explain the possible reaction mechanism.