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<p>The alkylation of phenol with styrene afforded a mixture of diastereomers of 2,6-bis-(α-methylbenzyl)phenol, which was separated by the O-acylation and subsequent chromatography of the resulting derivatives. The structures and relative configurations of the individual diastereomers were established by X-ray diffraction analysis of their O-acyl derivatives.</p>

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Diastereomers of 2,6-bis(α-methylbenzyl)phenol: synthesis and separation

  • 期刊论文

  • 发表日期：

    2025年12月1日

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  • I. Yu. Chukicheva,
  • I. V. Fedorova,
  • P. S. Tumaeva,
  • K. Yu. Suponitsky,
  • A. V. Kutchin

摘要

The alkylation of phenol with styrene afforded a mixture of diastereomers of 2,6-bis-(α-methylbenzyl)phenol, which was separated by the O-acylation and subsequent chromatography of the resulting derivatives. The structures and relative configurations of the individual diastereomers were established by X-ray diffraction analysis of their O-acyl derivatives.