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<p>The [4+2]-cycloaddition of maleic anhydride to 2-tropylcyclohexanone was studied and demonstrated to afford a mixture of <i>endo</i>- and <i>exo</i>-adducts in a 7: 1 ratio in a 90% total yield. The adducts were isolated in the individual state and their structures were established by modern 1D and 2D NMR spectroscopic methods and X-ray diffraction analysis.</p>

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Synthesis and X-ray diffraction analysis of diene adducts of 2-tropylcyclohexanone with maleic anhydride

  • 期刊论文

  • 发表日期：

    2025年3月1日

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  • G. N. Kadikova,
  • E. S. Meshcheryakova,
  • L. M. Khalilov

摘要

The [4+2]-cycloaddition of maleic anhydride to 2-tropylcyclohexanone was studied and demonstrated to afford a mixture of endo- and exo-adducts in a 7: 1 ratio in a 90% total yield. The adducts were isolated in the individual state and their structures were established by modern 1D and 2D NMR spectroscopic methods and X-ray diffraction analysis.