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<p>Malonates bearing 1,3-dioxacycloakane moiety were synthesized and some of their reactions were carried out under conditions of conventional heating and microwave irradiation. New malonates can be successfully used as C—H acids in the alkylation reaction as well as for the synthesis of tertiary amines and olefins. The conditions for synthesizing target products in quantitative yields using microwave activation were developed.</p>

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Synthesis and reactions of malonic esters based on hydroxymethyl-1,3-dioxacycloalkanes

  • 期刊论文

  • 发表日期：

    2025年2月1日

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  • Yu. G. Borisova,
  • R. M. Sultanova,
  • S. S. Zlotsky

摘要

Malonates bearing 1,3-dioxacycloakane moiety were synthesized and some of their reactions were carried out under conditions of conventional heating and microwave irradiation. New malonates can be successfully used as C—H acids in the alkylation reaction as well as for the synthesis of tertiary amines and olefins. The conditions for synthesizing target products in quantitative yields using microwave activation were developed.