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<p>Trimethylsilyl (1-trimethylsilyl-1<i>H</i>-indol-3-yl)acetate, (chloromethyl)(dimethyl)silyl (1<i>H</i>-indol-3-yl)acetate, and (chloromethyl)(dimethyl)silyl [1-(chloromethyl)(dimethyl)-silyl-1<i>H</i>-indol-3-yl]acetate were synthesized by silylation of 1<i>H</i>-indole-3-acetic acid with hexamethyldisilazane, Me<sub>3</sub>SiCl, and ClCH<sub>2</sub>SiMe<sub>2</sub>Cl. The structures of obtained compounds were confirmed by multinuclear NMR spectroscopy and IR spectroscopy.</p>

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Synthesis of silyl derivatives of 1H-indole-3-acetic acid

  • 期刊论文

  • 发表日期：

    2025年6月1日

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  • A. S. Soldatenko,
  • A. I. Albanov,
  • N. F. Lazareva

摘要

Trimethylsilyl (1-trimethylsilyl-1H-indol-3-yl)acetate, (chloromethyl)(dimethyl)silyl (1H-indol-3-yl)acetate, and (chloromethyl)(dimethyl)silyl [1-(chloromethyl)(dimethyl)-silyl-1H-indol-3-yl]acetate were synthesized by silylation of 1H-indole-3-acetic acid with hexamethyldisilazane, Me3SiCl, and ClCH2SiMe2Cl. The structures of obtained compounds were confirmed by multinuclear NMR spectroscopy and IR spectroscopy.