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<p>Conditions for mono-, di-, and triazidation of 1,3,5-trifluoro-2,4,6-triiodobenzene with sodium azide were developed varying solvents, temperature, and molar ratio of reactants to furnish 1-azido-3,5-difluoro-2,4,6-triiodobenzene, 1,3-diazido-5-fluoro-2,4,6-triiodobenzene, and 1,3,5-triazido-2,4,6-triiodobenzene, which can be used as precursors for photochemical synthesis of triiodinated mono-, di-, and trinitrenes.</p>

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Mono-, di-, and triazidation of 1,3,5-trifluoro-2,4,6-triiodobenzene

  • 期刊论文

  • 发表日期：

    2025年6月1日

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  • I. K. Yakushchenko,
  • S. V. Chapyshev

摘要

Conditions for mono-, di-, and triazidation of 1,3,5-trifluoro-2,4,6-triiodobenzene with sodium azide were developed varying solvents, temperature, and molar ratio of reactants to furnish 1-azido-3,5-difluoro-2,4,6-triiodobenzene, 1,3-diazido-5-fluoro-2,4,6-triiodobenzene, and 1,3,5-triazido-2,4,6-triiodobenzene, which can be used as precursors for photochemical synthesis of triiodinated mono-, di-, and trinitrenes.