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15N-Labeled tetrazoloazines in investigation of the azido-tetrazole equilibrium

  • S. L. Deev,
  • E. S. Sheina,
  • T. S. Shestakova,
  • V. N. Charushin,
  • O. N. Chupakhin

摘要

The data on studying the azido-tetrazole equilibrium in the tetrazoloazine series by using 15N-labeled samples are reviewed. The incorporation of the 15N atom significantly expands capabilities of NMR spectroscopy. An analysis of chemical shifts and 1H—15N, 13C—15N, and 15N—15N spin-spin coupling constants is an efficient method for studying these transformations.