CuI nanoparticles immobilized on Fe3O4@SiO2@2,2′-bipyridine: an efficient catalyst for 1,2,3‐triazoles synthesis
摘要
In this context, we introduced the immobilization of CuI nanoparticles on to the surface of 2,2′-bipyridine functionalized magnetic nanoparticles to create a heterogeneous catalytic system [Fe3O4@SiO2@2,2′-BP@CuI NPs]. After characterization of prepared hybrid structure by using suitable methods such as Fourier-transform infrared spectroscopy (FTIR), thermogravimetric/derivative thermogravimetry (TG/DTG), X-ray diffraction (XRD), energy-dispersive X-ray spectroscopy (EDS), field-emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), and vibrating-sample magnetometer (VSM), its catalytic behavior for the preparation of 1,2,3‐triazoles derivatives has been analyzed. Also, recovering and reusing behavior of Fe3O4@SiO2@2,2′-BP@CuI NPs show promising results of four runs while only a slight decrease in the performance of the catalyst was observed.