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Ultraslow calorimetric studies of the martensitic transformation of NiFeGa alloys: detection and analysis of avalanche phenomena

  • José-María Martín-Olalla,
  • Antonio Vidal-Crespo,
  • Francisco Javier Romero,
  • Alejandro F. Manchón-Gordón,
  • Jhon J. Ipus,
  • Javier S. Blázquez,
  • María Carmen Gallardo,
  • Clara F. Conde

摘要

We study the thermal properties of a bulk \(\hbox {Ni}_{55}\hbox {Fe}_{19}\hbox {Ga}_{26}\) Ni 55 Fe 19 Ga 26 Heusler alloy in a conduction calorimeter. At slow heating and cooling rates ( \(\sim {1}\,\hbox {K h}^{-1}\) 1 K h - 1 ), we compare as-cast and annealed samples. We report a smaller thermal hysteresis after the thermal treatment due to the stabilization of the 14 M modulated structure in the martensite phase. In ultraslow experiments ( \({40}\,\hbox {mK h}^{-1}\) 40 mK h - 1 ), we detect and analyze the calorimetric avalanches associated with the direct and reverse martensitic transformation from cubic to 14 M phase. This reveals a distribution of events characterized by a power law with exponential cutoff \(p(u)\propto u^{-\varepsilon }\exp (-u/\xi )\) p ( u ) u - ε exp ( - u / ξ ) where \(\varepsilon \sim 2\) ε 2 and damping energies \(\xi ={370}{\upmu {\rm J}}\) ξ = 370 μ J (direct) and \(\xi ={27}{\upmu {\rm J}}\) ξ = 27 μ J (reverse) that characterize the asymmetry of the transformation.