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<p>This study successfully anchored palladium onto the surface of organically modified g-C<sub>3</sub>N<sub>4</sub> using a simple and cost-efficient method. The resulting nanocatalyst demonstrated durability and high efficiency as a nano-reactor for synthesizing tetrazole derivatives. Comprehensive characterization of this eco-friendly heterogeneous catalyst was performed using various techniques, including Fourier transform infrared spectroscopy, scanning electron microscopy, energy-dispersive X-ray spectroscopy, inductively coupled plasma optical emission spectroscopy, X-ray diffraction, thermal gravimetric analysis, and nitrogen adsorption-desorption. Notable advantages of this methodology include the use of a green medium, straightforward separation and workup procedures, excellent reusability of the nanocatalyst, and shorter reaction times.</p>

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Palladium nanoparticles supported on exfoliated g-C3N4 as efficient catalysts for one-pot synthesis of 5-substituted 1 H-tetrazoles

  • 期刊论文

  • 发表日期：

    2026年2月12日

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  • Nafis Ahmad,
  • Rima Heider Al Omari,
  • G. PadmaPriya,
  • Baraa Mohammed Yaseen,
  • Y. Sasikumar,
  • Renu Sharma,
  • Abhayveer Singh,
  • Rasul Usmanov,
  • Khushnud Azizjanov

摘要

This study successfully anchored palladium onto the surface of organically modified g-C3N4 using a simple and cost-efficient method. The resulting nanocatalyst demonstrated durability and high efficiency as a nano-reactor for synthesizing tetrazole derivatives. Comprehensive characterization of this eco-friendly heterogeneous catalyst was performed using various techniques, including Fourier transform infrared spectroscopy, scanning electron microscopy, energy-dispersive X-ray spectroscopy, inductively coupled plasma optical emission spectroscopy, X-ray diffraction, thermal gravimetric analysis, and nitrogen adsorption-desorption. Notable advantages of this methodology include the use of a green medium, straightforward separation and workup procedures, excellent reusability of the nanocatalyst, and shorter reaction times.