This study aims to identify the electromagnetic wave conduction capability of steel-fiber reinforced C-30/37 concrete and autoclaved aerated (or foamed) concrete, which are commonly used in Türkiye, for the \(400\) to \(2400\) MHz band to make provisions for penetration depth at these frequency ranges. Transmission-only \({\text{S}}_{21}\) measurement results in free-space are presented for different material thicknesses. Multipath propagation effects are mitigated using an accurate gating scheme in the time domain. Two characterization techniques are proposed: direct attenuation estimation from the measured data and complex permittivity estimation using low-loss dielectric approximation. Both techniques yield almost identical attenuation results, showing a significant variation over the studied frequency band. Results indicate that signal attenuation ranges from \(26\) dB/m at \(400\) MHz to \(66\) dB/m at \(2400\) MHz for C-30/37 concrete whereas these numbers are measured as \(33\) dB/m at \(400\) MHz and \(58\) dB/m at \(2400\) MHz for aerated concrete. Proposed analysis methods can be quantitatively very useful and employed accurately, especially for determining and estimating the dielectric and conductive parameters of any homogeneous material. Based on these findings, the results of power budget analyses and exemplary radar experiments are presented and evaluated to determine the limits of the applicability of detecting and locating a living person behind such materials.