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<p>This study presents a novel method for quickly preparing nanoscale SnO<sub>2</sub> materials through a low-heat solid-state reaction. This method utilizes SnSO<sub>4</sub> and H<sub>2</sub>O<sub>2</sub> disinfectant powder (H<sub>2</sub>O<sub>2</sub> as a reactive substance) as raw materials. When the mixed powders were heated to 90&#xa0;°C, a rapid reaction occurred, which resulted in the formation of SnO<sub>2</sub>. X-ray diffraction results showed that the prepared SnO<sub>2</sub> material was amorphous, The powder exhibited good dispersion, and SnO<sub>2</sub> nanoparticles were approximately 20&#xa0;nm in size. X-ray photoelectron spectroscopy results revealed that the sample surface was rich in hydroxyl. Finally, a reaction mechanism for preparing nanoscale SnO<sub>2</sub> materials through a solid-state reaction was proposed.</p>

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A New Approach to Synthesize Nano-Sized SnO2 Via Low Temperature Solid-State Reaction

  • 期刊论文

  • 发表日期：

    2025年4月5日

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  • He Zhao,
  • Bocheng Meng,
  • Yanhong Wang,
  • Shikai Zhao

摘要

This study presents a novel method for quickly preparing nanoscale SnO2 materials through a low-heat solid-state reaction. This method utilizes SnSO4 and H2O2 disinfectant powder (H2O2 as a reactive substance) as raw materials. When the mixed powders were heated to 90 °C, a rapid reaction occurred, which resulted in the formation of SnO2. X-ray diffraction results showed that the prepared SnO2 material was amorphous, The powder exhibited good dispersion, and SnO2 nanoparticles were approximately 20 nm in size. X-ray photoelectron spectroscopy results revealed that the sample surface was rich in hydroxyl. Finally, a reaction mechanism for preparing nanoscale SnO2 materials through a solid-state reaction was proposed.