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<p>The compound 1,4,7-trithia-10,13-diazacyclopentadecane-9,14-dione, <b>1</b>, crystallizes in the space group <i>P</i>2<sub>1</sub>/<i>c</i> with <i>a</i> = 9.3608(3) Å, <i>b</i> = 16.0333(5) Å, <i>c</i> = 9.5608(3) Å, <i>β</i> = 113.3521(14)°, and <i>Z</i> = 4. The title molecule forms chains via face-to-face N–H<sup>…</sup>O hydrogen bonds. The structure of <b>1</b> is also compared to the previously reported oxygen analog, 1,4,7-trioxa-10,13-diazacyclopentadecane-9,14-dione.</p>

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Crystal Structure Analysis of 1, 4, 7-Trithia-10, 13-diazacyclopentadecane-9, 14-dione

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  • 发表日期：

    2025年6月12日

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  • Timothy M.E. Jugovic,
  • Christopher G. Hamaker

摘要

The compound 1,4,7-trithia-10,13-diazacyclopentadecane-9,14-dione, 1, crystallizes in the space group P21/c with a = 9.3608(3) Å, b = 16.0333(5) Å, c = 9.5608(3) Å, β = 113.3521(14)°, and Z = 4. The title molecule forms chains via face-to-face N–H…O hydrogen bonds. The structure of 1 is also compared to the previously reported oxygen analog, 1,4,7-trioxa-10,13-diazacyclopentadecane-9,14-dione.