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<p>Pure zinc oxide nanoparticles (NPs) and its nanocomposite ZnO/Lu<sub>2</sub>O<sub>3</sub> NPs with Zn/Lu varied weight ratios (Zn/Lu; 97:3, 94:6, and 91:9%) were produced using a precipitation process under optimal circumstances. The synthesized samples were analyzed using diffraction of X-ray, scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy, transmission electron microscopy (TEM), and Raman spectra. The ZnO NPs as-prepared possess a highly crystalline structure of wurtzite ZnO and great phase purity. The combined Lu<sub>2</sub>O<sub>3</sub> and ZnO NPs show a Lu<sub>2</sub>O<sub>3</sub> zinc blend phase as well as the pure ZnO’s wurtzite phase, proving the samples’ excellent purity and crystallinity as-prepared. Increasing the Lu<sub>2</sub>O<sub>3</sub> percentage to 9% resulted in a considerable drop in the surface area of ZnO samples from 29.9 to 8.4&#xa0;m<sup>2</sup>/g and the volume of the pore from 0.3536 to 0.020&#xa0;cm<sup>3</sup>/g, according to nitrogen adsorption–desorption studies. The study found that adding Lu<sub>2</sub>O<sub>3</sub> NPs improves the photocatalytic capabilities of ZnO NPs for methylene blue degradation. Mixed 9% Lu<sub>2</sub>O<sub>3</sub> and 91% ZnO NPs have much higher photocatalytic activity than pure ZnO NPs due to their high crystallinity and small energy gap.</p>

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Fabrication of a novel ZnO/Lu2O3 nanomaterial for the photocatalytic disposal of methylene blue dye under solar cell illumination

  • 期刊论文

  • 发表日期：

    2025年2月15日

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  • Wael. H. Alsaedi,
  • Ateyatallah Aljuhani,
  • M. Alahmadi,
  • Hamza Qassium,
  • Belal H. M. Hussein,
  • Majed O. Alawad,
  • M. Khushaim,
  • Ahmed M. Abu-Dief

摘要

Pure zinc oxide nanoparticles (NPs) and its nanocomposite ZnO/Lu2O3 NPs with Zn/Lu varied weight ratios (Zn/Lu; 97:3, 94:6, and 91:9%) were produced using a precipitation process under optimal circumstances. The synthesized samples were analyzed using diffraction of X-ray, scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy, transmission electron microscopy (TEM), and Raman spectra. The ZnO NPs as-prepared possess a highly crystalline structure of wurtzite ZnO and great phase purity. The combined Lu2O3 and ZnO NPs show a Lu2O3 zinc blend phase as well as the pure ZnO’s wurtzite phase, proving the samples’ excellent purity and crystallinity as-prepared. Increasing the Lu2O3 percentage to 9% resulted in a considerable drop in the surface area of ZnO samples from 29.9 to 8.4 m2/g and the volume of the pore from 0.3536 to 0.020 cm3/g, according to nitrogen adsorption–desorption studies. The study found that adding Lu2O3 NPs improves the photocatalytic capabilities of ZnO NPs for methylene blue degradation. Mixed 9% Lu2O3 and 91% ZnO NPs have much higher photocatalytic activity than pure ZnO NPs due to their high crystallinity and small energy gap.