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<p>In this study, we report the design and preparation of an innovative palladium-based nanocatalyst, where palladium is anchored on phosphine-functionalized magnetic nanoparticles coated with an ionic liquid (IL) layer. This material is applied in the Suzuki–Miyaura cross-coupling reaction, performing efficiently at room temperature in a green ethanol–water solvent system with low palladium loading. It successfully catalyzes structurally different aryl halides and boronic acids, providing excellent yields under mild, air-tolerant conditions. Comprehensive characterization confirms the catalyst’s robust structure, and recyclability tests demonstrate its durability across multiple uses without significant performance loss.</p>

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Palladium on ionic liquid–phosphine-modified magnetic nanoparticles for aqueous Suzuki–Miyaura reaction at room temperature

  • 期刊论文

  • 发表日期：

    2025年12月14日

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  • Mohammad Gholinejad,
  • Maryam Heidary,
  • José M. Sansano

摘要

In this study, we report the design and preparation of an innovative palladium-based nanocatalyst, where palladium is anchored on phosphine-functionalized magnetic nanoparticles coated with an ionic liquid (IL) layer. This material is applied in the Suzuki–Miyaura cross-coupling reaction, performing efficiently at room temperature in a green ethanol–water solvent system with low palladium loading. It successfully catalyzes structurally different aryl halides and boronic acids, providing excellent yields under mild, air-tolerant conditions. Comprehensive characterization confirms the catalyst’s robust structure, and recyclability tests demonstrate its durability across multiple uses without significant performance loss.