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Synthesis and Structural Study of Cytisinylphenylacetic Acid Nitriles

  • D. S. Ismailova,
  • U. S. Makhmudov,
  • Kh. M. Bobakulov,
  • B. Zh. Elmuradov,
  • A. A. Kadirov,
  • Kh. M. Shakhidoyatov,
  • B. Tashkhodzhaev

摘要

Nitriles of stereoisomeric cytisinylarylacetic acids were synthesized by reacting cytisine with aromatic aldehydes in the presence of acetone cyanohydrin. Nitriles of cytisinylphenylacetic acids with the R- and S-configuration of the arylacetonitrile fragment were shown to be formed regioselectively in basic solution. The absolute configurations of the synthesized products were established using NMR spectroscopy and X-ray crystal structure analyses.