<p>Besides solid solution strengthening, microstructural refinement is another approach that can enhance the mechanical strength of high entropy alloys. This can be achieved using the high cooling rates inherent to the laser surface remelting process. In this work, the surface of a novel arc-melted Cr<sub>35</sub>Mn<sub>5</sub>Fe<sub>5</sub>Co<sub>5</sub>Ni<sub>50</sub> (%at.) alloy was modified by laser surface remelting. Two laser powers were used in this work, 200 W and 300 W, to study the influence of heat input on the resulting microstructure. A fixed laser scanning velocity of 11.6&#xa0;mm/s was used. Microstructural characterization was performed using X-ray diffraction, optical microscopy, and scanning electron microscopy. Electron backscattered diffraction analysis was also used to evaluate grain size and crystallographic orientation in the remelted surfaces. The laser tracks showed significant grain size refinement in comparison to the substrate. The laser track processed with the lower laser power (200 W) had the most refined microstructure, with an average grain size of 23&#xa0;μm. The laser track processed with the higher laser power (300 W) showed an average grain size of 54&#xa0;μm. The substrate displayed an average grain size larger than 200&#xa0;μm. A significant increase in microhardness, from 160 ± 5 HV (substrate) to 189 ± 10 HV (200 W) and 196 ± 4 HV (300 W), was observed in the laser track areas, which is attributed to the significant microstructural refinement obtained in the remelted areas.</p>

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Microstructural evolution and hardness enhancement in a novel Cr-Mn-Fe-Co–Ni high entropy alloy processed by laser surface remelting

  • Maria Helena Teles Lopes,
  • Adilson Vitor Rodrigues,
  • Pablo Miguel de Souza,
  • Guilherme Cardeal Stumpf,
  • Eric Marchezini Mazzer,
  • Francisco Gil Coury,
  • Andres Felipe Ramirez,
  • João Batista Fogagnolo,
  • Pedro Henrique Rodrigues Pereira,
  • Witor Wolf

摘要

Besides solid solution strengthening, microstructural refinement is another approach that can enhance the mechanical strength of high entropy alloys. This can be achieved using the high cooling rates inherent to the laser surface remelting process. In this work, the surface of a novel arc-melted Cr35Mn5Fe5Co5Ni50 (%at.) alloy was modified by laser surface remelting. Two laser powers were used in this work, 200 W and 300 W, to study the influence of heat input on the resulting microstructure. A fixed laser scanning velocity of 11.6 mm/s was used. Microstructural characterization was performed using X-ray diffraction, optical microscopy, and scanning electron microscopy. Electron backscattered diffraction analysis was also used to evaluate grain size and crystallographic orientation in the remelted surfaces. The laser tracks showed significant grain size refinement in comparison to the substrate. The laser track processed with the lower laser power (200 W) had the most refined microstructure, with an average grain size of 23 μm. The laser track processed with the higher laser power (300 W) showed an average grain size of 54 μm. The substrate displayed an average grain size larger than 200 μm. A significant increase in microhardness, from 160 ± 5 HV (substrate) to 189 ± 10 HV (200 W) and 196 ± 4 HV (300 W), was observed in the laser track areas, which is attributed to the significant microstructural refinement obtained in the remelted areas.